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Techniques and Experiments for Organic Chemistry

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Description:Techniques and Experiments for Organic Chemistry begins with the common laboratory techniques. Actual syntheses are postponed until the student has gained sufficient knowledge of organic chemistry from the lecture portion of the course to understand the experiments being performed. Synthetic work follows the technique chapters of the text and begins with alkyl halide chemistry (Williamson ether synthesis and a Grignard reaction), followed by alcohol chemistry. Spectral techniques (infrared and NMR) are placed after alcohol chemistry, approximately halfway through the text. The remaining chapters are devoted to additional synthetic procedures. The text ends with a chapter on the literature of organic chemistry, an introduction to organic qualitative analysis, and a chapter of supplemental techniques. Four appendices of assorted tables and laboratory calculations conclude the text.Contents:1. The Organic Laboratory2. Melting Points- Experiment 2.1 Melting Points of Benzoic Acid and an Unknown- Experiment 2.2 Mixed Melting Points of Benzoic Acid and 2-Naphthol- Experiment 2.3 A Temperature-Dependent Liquid Crystal Display3. Crystallization- Experiment 3.1 Crystallization of Benzoic Acid and an Unknown- Experiment 3.2 Crystallization of Acetanilide Using Decolorizing Charcoal4. Extraction- Experiment 4.1 Extraction of Adipic Acid and an Unknown from Water--A Quantitative Study- Experiment 4.2 Chemically Active Extraction- Experiment 4.3 Extraction of Caffeine from Tea5. Distillation- Experiment 5.1 Simple Distillation- Experiment 5.2 Fractional Distillation- Experiment 5.3 Fractional Distillation of an Unknown Mixture6. Introduction to Chromatography; Thin-Layer Chromatography- Experiment 6.1 Thin-Layer Chromatography of Analgesic Drugs7. Gas-Liquid Chromatography- Experiment 7.1 GLC Analysis of a Mixture- Experiment 7.2 Quantitative GLC Analysis of a Mixture- Experiment 7.3 GLC Analysis of Distillation Fractions from Experiments 5.1 and 5.28. Substitution Reactions of Alkyl Halides- Experiment 8.1 Synthesis of n-Butyl Methyl Ether- Experiment 8.2 Solvent Effects in an Sn1 Solvolysis Reaction: A Kinetics Study9. The Grignard Reaction- Experiment 9.1 Synthesis of 2-Methyl-2-Hexanol: A Grignard Reaction10. The Chemistry of Alcohols- Experiment 10.1 Synthesis of 1-Bromobutane from 1-Butanol- Experiment 10.2 Synthesis of t-Butyl Chloride from t-Butyl Alcohol- Experiment 10.3 Synthesis of Cyclohexene by the Dehydration of Cyclohexanol- Experiment 10.4 Synthesis of Cyclohexanone by the Oxidation of Cyclohexanol11. Infrared Spectroscopy- Experiment 11.1 Infrared Spectra in Structure Determination12. Nuclear Magnetic Resonance Spectroscopy- Experiment 12.1 NMR Spectra in Structure Determination13. The Chemistry of Alkenes- Experiment 13.1 Synthesis of Cyclohexanol from Cyclohexene- Experiment 13.2 Synthesis of cis-1,2-Cyclohexanediol from Cyclohexene- Experiment 13.3 Synthesis of 9,10-Dihydroanthracene-9,10-endo-α,β-succinic Anhydride: A Diels-Alder Reaction- Experiment 13.4 Synthesis of Polystyrene14. Aromatic Substitution Reactions- Experiment 14.1 Synthesis of p-Nitroacetanilide from Acetanilide- Experiment 14.2 Synthesis of Methyl m-Nitrobenzoate from Methyl Benzoate- Experiment 14.3 Synthesis of Sulfanilamide: A Multistep Procedure15. The Chemistry of Aldehydes and Ketones- Experiment 15.1 Sodium Borohydride Reduction of Acetophenone- Experiment 15.2 Synthesis of Dixanthylene, a Thermochromic Compound16. The Chemistry of Carboxylic Acids and their Derivatives- Experiment 16.1 Saponification of Methyl Benzoate- Experiment 16.2 Hydrolysis of p-Nitroacetanilide- Experiment 16.3 Synthesis of Aspirin- Experiment 16.4 Synthesis of an Acetate Ester by a General Reaction Procedure- Experiment 16.5 Synthesis of Nylon 10,6: The "Nylon Rope Trick"17. Stereochemistry- Experiment 17.1 Cis,trans Isomerization of 1,2-Dibenzoylethylene- Experiment 17.2 Resolution of α-Phenylethylamine18. Enolate Condensations- Experiment 18.1 Synthesis of Dibenzalacetone- Experiment 18.2 Synthesis of (E)- and (Z)-α-Phenylcinnamic Acids19. Plant Products- Experiment 19.1 Isolation of Eugenol from Cloves; Synthesis of Eugenol Benzoate- Experiment 19.2 Isolation of Trimyristin from Nutmeg20. Introduction to the Chemical Literature21. Introduction to Qualitative Organic Analysis- Experiment 21.1 Qualitative Organic Analysis: Selected Procedures22. Supplemental Techniques- Experiment 22.1 Vacuum Distillation of Benzaldehyde- Experiment 22.2 Column Chromatography: Separation of...We have made it easy for you to find a PDF Ebooks without any digging. And by having access to our ebooks online or by storing it on your computer, you have convenient answers with Techniques and Experiments for Organic Chemistry. To get started finding Techniques and Experiments for Organic Chemistry, you are right to find our website which has a comprehensive collection of manuals listed.
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Pages: 449

Format: PDF, EPUB & Kindle Edition

Publisher: —

Release: 1983

ISBN: 0871507552

Description: Techniques and Experiments for Organic Chemistry begins with the common laboratory techniques. Actual syntheses are postponed until the student has gained sufficient knowledge of organic chemistry from the lecture portion of the course to understand the experiments being performed. Synthetic work follows the technique chapters of the text and begins with alkyl halide chemistry (Williamson ether synthesis and a Grignard reaction), followed by alcohol chemistry. Spectral techniques (infrared and NMR) are placed after alcohol chemistry, approximately halfway through the text. The remaining chapters are devoted to additional synthetic procedures. The text ends with a chapter on the literature of organic chemistry, an introduction to organic qualitative analysis, and a chapter of supplemental techniques. Four appendices of assorted tables and laboratory calculations conclude the text.Contents:1. The Organic Laboratory2. Melting Points- Experiment 2.1 Melting Points of Benzoic Acid and an Unknown- Experiment 2.2 Mixed Melting Points of Benzoic Acid and 2-Naphthol- Experiment 2.3 A Temperature-Dependent Liquid Crystal Display3. Crystallization- Experiment 3.1 Crystallization of Benzoic Acid and an Unknown- Experiment 3.2 Crystallization of Acetanilide Using Decolorizing Charcoal4. Extraction- Experiment 4.1 Extraction of Adipic Acid and an Unknown from Water--A Quantitative Study- Experiment 4.2 Chemically Active Extraction- Experiment 4.3 Extraction of Caffeine from Tea5. Distillation- Experiment 5.1 Simple Distillation- Experiment 5.2 Fractional Distillation- Experiment 5.3 Fractional Distillation of an Unknown Mixture6. Introduction to Chromatography; Thin-Layer Chromatography- Experiment 6.1 Thin-Layer Chromatography of Analgesic Drugs7. Gas-Liquid Chromatography- Experiment 7.1 GLC Analysis of a Mixture- Experiment 7.2 Quantitative GLC Analysis of a Mixture- Experiment 7.3 GLC Analysis of Distillation Fractions from Experiments 5.1 and 5.28. Substitution Reactions of Alkyl Halides- Experiment 8.1 Synthesis of n-Butyl Methyl Ether- Experiment 8.2 Solvent Effects in an Sn1 Solvolysis Reaction: A Kinetics Study9. The Grignard Reaction- Experiment 9.1 Synthesis of 2-Methyl-2-Hexanol: A Grignard Reaction10. The Chemistry of Alcohols- Experiment 10.1 Synthesis of 1-Bromobutane from 1-Butanol- Experiment 10.2 Synthesis of t-Butyl Chloride from t-Butyl Alcohol- Experiment 10.3 Synthesis of Cyclohexene by the Dehydration of Cyclohexanol- Experiment 10.4 Synthesis of Cyclohexanone by the Oxidation of Cyclohexanol11. Infrared Spectroscopy- Experiment 11.1 Infrared Spectra in Structure Determination12. Nuclear Magnetic Resonance Spectroscopy- Experiment 12.1 NMR Spectra in Structure Determination13. The Chemistry of Alkenes- Experiment 13.1 Synthesis of Cyclohexanol from Cyclohexene- Experiment 13.2 Synthesis of cis-1,2-Cyclohexanediol from Cyclohexene- Experiment 13.3 Synthesis of 9,10-Dihydroanthracene-9,10-endo-α,β-succinic Anhydride: A Diels-Alder Reaction- Experiment 13.4 Synthesis of Polystyrene14. Aromatic Substitution Reactions- Experiment 14.1 Synthesis of p-Nitroacetanilide from Acetanilide- Experiment 14.2 Synthesis of Methyl m-Nitrobenzoate from Methyl Benzoate- Experiment 14.3 Synthesis of Sulfanilamide: A Multistep Procedure15. The Chemistry of Aldehydes and Ketones- Experiment 15.1 Sodium Borohydride Reduction of Acetophenone- Experiment 15.2 Synthesis of Dixanthylene, a Thermochromic Compound16. The Chemistry of Carboxylic Acids and their Derivatives- Experiment 16.1 Saponification of Methyl Benzoate- Experiment 16.2 Hydrolysis of p-Nitroacetanilide- Experiment 16.3 Synthesis of Aspirin- Experiment 16.4 Synthesis of an Acetate Ester by a General Reaction Procedure- Experiment 16.5 Synthesis of Nylon 10,6: The "Nylon Rope Trick"17. Stereochemistry- Experiment 17.1 Cis,trans Isomerization of 1,2-Dibenzoylethylene- Experiment 17.2 Resolution of α-Phenylethylamine18. Enolate Condensations- Experiment 18.1 Synthesis of Dibenzalacetone- Experiment 18.2 Synthesis of (E)- and (Z)-α-Phenylcinnamic Acids19. Plant Products- Experiment 19.1 Isolation of Eugenol from Cloves; Synthesis of Eugenol Benzoate- Experiment 19.2 Isolation of Trimyristin from Nutmeg20. Introduction to the Chemical Literature21. Introduction to Qualitative Organic Analysis- Experiment 21.1 Qualitative Organic Analysis: Selected Procedures22. Supplemental Techniques- Experiment 22.1 Vacuum Distillation of Benzaldehyde- Experiment 22.2 Column Chromatography: Separation of...We have made it easy for you to find a PDF Ebooks without any digging. And by having access to our ebooks online or by storing it on your computer, you have convenient answers with Techniques and Experiments for Organic Chemistry. To get started finding Techniques and Experiments for Organic Chemistry, you are right to find our website which has a comprehensive collection of manuals listed.
Our library is the biggest of these that have literally hundreds of thousands of different products represented.

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Techniques and Experiments for Organic Chemistry

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